|
||
All probe microscopes have two features common features : a) a sharp, tiny probe gets very close to the sample and feels the surface by monitoring some kind of interaction, between the probe and the surface, which is very sensitive to distance. B) the sample or the probe is scanned in a rastor fashion with near atomic accuracy and the variation in the interaction is translated to a topographic map of the surface.
Among the family of SPM's the two most commonly used are Scanning Tunneling Microscopy (STM) and Atomic Force Microscopy (AFM). In STM, a sharp metallic probe and a conducting sample are brought together until their electronic wave functions overlap. By applying a potential bias between them, a tunneling current is produced. The probe is mounted on a piezoelectric drive that scans the surface. Combining the piezoelectric drive with a feedback loop allows imaging of the surface in either a constant current or a constant-height mode. In AFM, the probe tip is attached to a cantilever with a small spring constant. The probe is much like a spring which changes dimension upon experiencing a force ( Hookes' law) and the interaction that will be monitored is the repulsion between two atoms when they are brought extremely close to each other. The forces acting on the probe tip deflect the cantilever and the tip displacement is proportional to the force between the surface and the tip. The resultant bending of the AFM cantilever is measured optically by the deflection of the reflected laser beam. The most important advantage that AFM has over STM is that the former is not limited to conducting samples, so materials can often be imaged "as is" with essentially no sample preparation.
Using the above state-of-the-art nobel-prize winning (in 1986 for physics) technology, you will image two very familiar samples - a) the Compact Disk (CD) that we all use nearly everyday to listen to music and b) Graphite - a crystalline form of carbon that is in lead pencils that we write with. In the case of the CD you will be able to see the manner in which the musical information is stored. (the magnifications used will be of the order of 10,000). You will be able to compare this with the results on the cd obtained with the optical microscope and sem. You will also compare the surface features of the LP record using a profilometer. Fig.3 shows an AFM image of a CD stamper.
Figure 3. An atomic force microscope image of a CD stamper. The stamper has raised knobs that make tiny pits in the CD when it is stamped. These pits are scanned by the laser and the resulting digital signal is converted into an audio signal. The color coding above conveys the height of the knobs in nanometers (nm). The lower image is a 3-dimensional projection of a portion of the CD stamper.
Go Back to the Previous Page
Page authored by the ACEPT W3 Group Department of Physics and Astronomy, Arizona State University, Tempe, AZ 85287-1504 Copyright © 1995-2000 Arizona Board of Regents. All rights reserved. |